The Determination of Microamounts of Heavy Metals in Vegetable Oils by Differential Pulse Polarography
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چکیده
منابع مشابه
Selective Determination of Trace-Bismuth by Extraction-Differential Pulse Polarography in Non-Aqueous Media
The voltammetric characteristics of bismuth(III)-oxinate in chloroform at the mercury electrode were investigated and a quasi-reversible behavior for Bi(III) oxinate reduction was confirmed. Preceded by the extraction of Bi(III) oxinate in chloroform, differential pulse polarography was developed in the extracts for determination of the trace-bismuth. The linear range of the calibration gra...
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A simple and rapid differential pulse polarographic method was developed for the trace determination of azathioprine. A welldefined polarogram with three peaks was obtained in acetate buffer (pH 5.0) with peak potentials -0.27 V, -0.73 V and -1.02 V. The current-concentration linearity was found extend up to 5 x 10 mol L (r = 0.9992) with minimum detection limit of 2.8x10 mol L. The values of r...
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The method is based on the separation of Tl(I) as Tl(2)HPMo(12)O(40), stripping of the molybdate, and measurement of the peak current in differential-pulse polarography of the molybdenum. The calibration graph is linear over the range 2-12 ppm of thallium. The relative standard deviation is 1.2% (7 replicates each containing 500 microg of thallium). The current due to reduction of the molybdenu...
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Extractive Differential Pulse Polarography of Mo (VI) Oxinate in Chloroform and its Application in the Determination of Molybdenum in Steel
The voltammetric characteristics of Mo (VI) oxinate at the mercury electrode, in the presence of tri-butylammonium perchlorate (tri-BAP) and piperidinium perchlorate (PP) + piperidine (P) as two different types supporting electrolytes, have been studied in chloroform. With the both supporting electrolytes a two electron irreversible process for the reduction of Mo (VI) oxinate was observe...
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ژورنال
عنوان ژورنال: Journal of Japan Oil Chemists' Society
سال: 1978
ISSN: 1884-2003
DOI: 10.5650/jos1956.27.312